SYMPOSIUM ON NMR

POSTER SESSIONS

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A

Using 31P{1H} Cross Polarization MAS NMR to Probe the Surface Dissolution of Phosphate Glasses. Todd M. Alam and David P. Lang, Sandia National Laboratories

B

Location of Protons in Anhydrous Keggin Heteropolyacids by using 1H<->31P REDOR and Molecular Modeling. Alain Bailly, Jean-Francois Paul, Jean-Paul Amoureux, Michel Fournier, Michel Guelton, Université des Sciences et Technologies de Lille; Subramanian Ganapathy, University of Pune

A

Characterization of Bronsted acid sites in zeolites by MQ-REDOR NMR. Subramanian Ganapathy, University of Pune; Laurent Delevoye, Alain Bailly, Jean-Paul Amoureux, Université des Sciences et Technologies de Lille

B

Recent Developments of CP MAS between quadrupolar nuclei and spin 1/2. Jean-Paul Amoureux, Alain Bailly, Université des Sciences et Technologies de Lille; Marek Pruski, Iowa State University

A

Chemical Shift Tensors of Polycyclic Aromatic Molecules Determined by Magic Angle Turning. Dewey H. Barich; A. M. Orendt; J. Z. Hu; R. J. Pugmire; D. M. Grant; University of Utah

B

A 2H and 13C Experimental Solid-State NMR and Theoretical Study of Zeise's Salt, K[PtCls(C2H4)]@H2O. Guy M. Bernard; Roderick E. Wasylishen, Dalhousie University

A

Structure Determination of Peptides and Proteins Using Solid State NMR. Peter V. Bower; Joanna R. Long; Nathan A. Oyler; Gary P. Drobny, University of Washington

B

Magnetic Resonance Microimaging (MRM) of Petroleum Coke. Eric B. Brouwer, Yves Deslandes, Institute for Chemical Process and Environmental Technology (ICPET); Igor Moudrakovski, John A. Ripmeester, Steacie Institute for Molecular Sciences (SIMS); Keng H. Chung, Edmonton Research Centre

A

Experimental 9Be Solid-State NMR Study of Be(acac)2 and Theoretical Studies of 9Be Electric Field Gradient and Chemical Shielding Tensors. The First Evidence for Anisotropic Beryllium Shielding. David L. Bryce; Roderick E. Wasylishen, Dalhousie University

B

Remote Access to NMR Spectrometers at the EMSL DOE User Facility. Sarah Burton; Andrew Lipton, PNNL

A

Investigation of Local Structure Environment in Glasses by 17O, 23Na and 27Al MQ-MAS NMR. F. Angeli, T. Charpentier, P. Faucon, J.-C. Petit, J. Virlet, Service de Chimie Moléculaire, CEA Saclay

B

13C NMR Studies of the Selective Oxidation of n-Butane on Vanadium Phosphorus Oxide Catalysts. Bin Chen, Eric J. Munson, University of Minnesota

A

NMR Studies of 129Xe Diffusion in Ethylene-Propylene Copolymers. Naira M. da Silva, Maria Ines B. Tavares, Instituto de Macromoléculas Prof. Eloisa Mano, Universidade Federal do Rio de Janeiro; Hanna Gracz, E. O. Stejskal, North Carolina State University

B

NMR Spectroscopy and Solid Phase Synthesis: Polymer Signal Suppression via Isotropic Mixing in 1D Gel Phase 1H NMR Michael J.T. Ditty, R.M.E. Mainville and W.P. Power, University of Waterloo; H.N. Hunter, Brantford Chemicals Inc.

A

Solid-State NMR Characterization of 93Nb, 19F Spin Pairs in Niobium Fluorides and Oxyfluorides. Lin-Shu Du, Robert W. Schurko, Kwang Hun Lim and Clare P. Grey, SUNY at Stony Brook

B

Se NMR Measurements on Exceptional Se-As Glasses. Birgit Effey, D. A. Drabold, R. L. Cappelletti, Ohio University; J. R. Sachleben, Ohio State University

A

Phosphorus Chemical Shift Tensors for Tetramethyldiphosphine Disulfide - A 31P Single Crystal NMR, Dipolar-Chemical Shift NMR and Ab Initio Study. Myrlene Gee, Roderick E. Wasylishen and Klaus Eichele, Dalhousie University; James F. Britten, McMaster University

B

Applications of Toroid Cavity NMR Detectors to Metals, Polymers, Radioactive Materials, and Supercritical Fluids. Rex E. Gerald II, David E. Fremgen, Luis H. Nuñez, Donald T. Reed, Robert J. Klingler, Jerome W. Rathke, Argonne National Laboratory; Klaus Woelk, University of Bonn

A

Distribution of Crystalline and Amorphous Polymer Electrolyte in an Electrochemical Cell. Rex E. Gerald II, Edward T. Chainani, Robert J. Klingler, Jerome W. Rathke, Argonne National Laboratory

B

Rotational Sideband Separation at High Spinning Speeds: Applications to 207Pb, 139La and 93Nb NMR. James M. Gibson, Frederick G. Vogt, David J. Aurentz, Alan J. Benesi, Karl T. Mueller, Pennsylvania State University

A

Tin Composite Oxide Anode Materials as Probed by Multinuclear NMR, Diffraction and X-ray Absorbtion Spectroscopy. Gillian R. Goward, Linda F. Nazar, and William P. Power, University of Waterloo; Fabrice Leroux, Université Blaise-Pascal; Wojtek.Dmowski and Takeshi.Egami University of Pennsylvania

B

Passive-Shimming Designs of Toroid Cavity Probes using Spectral Distortion Parameters. Eric Growney, Rex Gerald II, Robert Klingler, Jerome Rathke, Argonne National Laboratory; Gary Friedman, University of Illinois at Chicago

A

Solid State NMR Study of Molecular Motion in Hexakis(trifluoromethyl)benzene. Edward W. Hagaman and David K. Murray, Oak Ridge National Laboratory

B

Solid-State NMR Analysis of Semiconductor Clusters and Thin Films. S.E. Hayes, L. Dinh, M. Balooch, Lawrence Livermore National Laboratory; J.A. Reimer, UC Berkeley

A

Surface and defect characterisation by 27Al NMR and PALS of intermediate phases formed during calcination of gibbsite, Al(OH)3, to corundum, a-Al2O3. Anita J.Hill, Timothy J.Bastow and Steven Celotto, CSIRO Manufacturing Science and Technology

B

Stochastic Wideline NMR Spectroscopy - Advantages, Problems and Solutions. Ole Hirsch, Friedrich Schiller University Jena, Institute for Optics and Quantum Electronics; Frank Weingarten, Rheinisch-Westfälische Technische Hochschule Aachen, Institute of Technical and Macromolecular Chemistry

A

Solid-State 25Mg and 93Nb NMR Studies of the formation of Lead Magnesium Niobate Pb(Mg1/3Nb2/3)O3. J. Huang, S. Prasad, J. Shore and J.J. firzgerald, South Dakota State University; H. Lock and G.E. Maciel, Colorado State University

B

Solid-State 13C NMR Investigation of Ring-Flipping Dynamics of Benzyl-Ether Dendritic Macromolecules, Joseph S. H. Huang and Christopher A. Klug, Stanford University

A

Solid-State 1H and 29Si NMR Studies of Hydrogen-Loaded and Ultraviolet-Irradiated Optical Fiber Materials. Margaret Hubbard, Erin Gill, and Sarah Gilbert, National Institute of Standards and Technology; Jincheng Xiong, Herman Lock, and Gary E. Maciel, Colorado State University

B

Development of Variable-Temperature Isolated Flow and Large Sample volume MAS NMR Probes for Heterogeneous Catalysis Studies. Lauren E. Kaune, Paul K. Isbester and Eric J. Munson, University of Minnesota

A

Solid-State NMR Studies of Tri-p-tolylamine/Polycarbonate Blends. Brian Kesling, Eric Hughes, and Terry Gullion, West Virginia University

B

87Rb MAS and MQMAS NMR Studies of High Temperature Phase Transitions in LiRbSO4. Hae Jin Kim, Marek Pruski, Jerzy W. Wiench, Iowa State University; Sung Ho Choh, Korea University

A

Solid-State 19F NMR Study of Molecular Dynamics of PFPE Lubricant Films on Amorphous Carbon Surfaces, Yoojin Kim and Christopher A. Klug, Stanford University

B

A 380 MHz Gyrotron-Based DNP Spectrometer, K.E. Kreischer, C.T. Farrar, R.G. Griffin, R.J. Temkin, J.R. Vieregg, MIT

A

Solid-State NMR Study of Exchanged Zeolites, Theresa A. Lalain, Karl T. Mueller, James R. Fehlner ,The Pennsylvania State University; D.E.W. Vaughan, Exxon Research and Engineering Company

B

Using 27Al, 31P MAS and 31P/27Al TRAPDOR NMR Spectroscopies to Study Sodium Aluminophosphate Glasses. David P. Lang and Todd M. Alam, Sandia National Laboratories

A

Solid-State Vanadium-51 NMR Studies of Dioxovanadate(V) Complexes. Man-Ho Lee, Kyungpook National University; Shigenobu Hayashi, National Institute of Materials and Chemical Research

B

Towards An Exact Solution To The Difficulties In REDOR For Multiply Coupled Heteronuclear Spin Systems. Oskar Liivak, David B. Zax, Cornell University

A

Analysis of the Multiple Quantum Cross Polarization NMR Experiment for 19F/23Na and 1H/27Al Spin Systems in Solids. Kwang Hun Lim and Clare P. Grey, SUNY Stony Brook

B

Experimental Investigation of the Possiblilities Open by Recent Sensitivity Improvements of the Quadrupolar MQ-MAS Experiment. Thomas Vosegaard, Pierre Florian, Valérie Montouillout, and Dominique Massiot; CNRS-CRMHT

A

Determination of Internuclear Distances from Solid-State NMR: Applications of Monte Carlo Error Analysis to REDOR Data. Sue M. Mattingly, Fredrick G. Vogt and Karl T. Mueller, The Pennsylvania State University; Leonard J. Mueller, University of California at Riverside

B

Identification of Histidyl and Lysyl Residues at a Potential Allosteric Site of Ribulose 1,5-Bisphosphate Carboxylase/Oxygenase. Lynda M. McDowell, Matthew E. Merritt, Jacob Schaefer, Washington University; Joe S. Schriner, Karinne Cortes, Delbert D. Mueller, Kansas State University

A

Heteronuclear 2D Local Field NMR Spectroscopy Under Fast MAS: Principles and Applications to Organic Solids. Dan McElheny, Enrico DeVita and Lucio Frydman, University of Illinois at Chicago

B

Distance Measurements to the Phosphosdiester Backbone of Nucleic Acids Using Solid-State NMR. Matthew E. Merritt, Gary A. J. Meints, Snorri Th. Sigurdsson, Gary P. Drobny, University of Washington

A

A Solid-State Deuterium NMR Study of DNA Methyltransferase Binding Sites: Effects of Methylation on Backbone and Furanose Ring Dynamics. Gary A. J. Meints, Gary P. Drobny, University of Washington; Karen B. Geahigan, 3M Chemicals; Mary E. Hatcher-Skeers, Claremont Colleges

B

Finite Pulse Widths and Infinite Linewidths: Echo Shapes and Relative Intensities. Joel B. Miller, Naval Research Laboratory

A

109Ag NMR Studies of Silver-Exchanged Zeolites. Igor L. Moudrakovski, Christopher I. Ratcliffe, John A. Ripmeester, Steacie Institute for Molecular Sciences (SIMS)

B

Quantification of Phosphorus-Chalcogen Bonding Preferences in Ternary Phosphorus-Sulfur-Selenium Glasses by Multiple-phase 31P and High-temperature 77Se NMR. Paul F. Mutolo, University of California at Santa Barbara; Hellmut Eckert, Institut für Physikalische Chemie, WWU

A

207Pb and 27Al Solid State NMR Studies of Lead-exchanged Zeolites. Heiko G. Niessen, Jeffrey A. Reimer, Alexis T. Bell, University of California Berkeley; C. Dybowski, University of Delaware; David R. Corbin, DuPont Company

B

Dynamic Nuclear Polarization in Aqueous Char Suspensions at 9.4 GHz. B.M.Odintsov, R.L.Belford, R.B.Clarkson, P.J.Ceroke, Illinois EPR Research Center; V.A.Atsarkin, V.N.Demidov, Institute of Radioengineering and Electronics

A

Spin-lattice Relaxation and Nmr Spectroscopy in Aqueous Char Suspensions. B.M.Odintsov, R.L.Belford, P.J.Ceroke, R.B.Clarkson, Illinois Research EPR Center; Z.Sh.Idiyatullin; A.N.Temnikov, State Technological University

B

Solid-State 27A1 MAS NMR Investigations of Aion Powders and Ceramics. Tom Offerdahl and John J. Fitzgerald, South Dakota State University; Steven F. Dec, Colorado School of Mines and Technology; Gary E. Maciel, Colorado State University

A

Determination of the Orientation of the Glycine-Alpha Carbon CSA Tensor in the Dipeptide AG. Nathan A. Oyler, John Stringer, and Gary P. Drobny, University of Washington

B

Comparison 13C CP/MAS NMR and Powder X-ray Diffraction for Analyzing Solid Organic Compounds. Brian E. Padden, Mark T. Zell, Zedong Dong, David J.W. Grant, Eric J. Munson, University of Minnesota; Steve A. Schroeder, The Monsanto Company

A

Investigations of Titanosilicate Materials by Solid-state 29Si and 47,49Ti NMR Spectroscopy. R.L. Peterson and J.J. Fitzgerald, South Dakota State University

B

Solution 13C, 47,49Ti and 93Nb NMR Studies of Titanate and Niobate Alkoxide Sol-Gel Precursors to Electronic Materials. J. Qi, J. Huang and J.J. Fitzgerald, South Dakota State University

A

NMR of Paramagnetic Lanthanide Glutarates. Joseph R. Sachleben, The Ohio State University; Anthony Cheetham, University of California Santa Barbara; Gérard Férey, Thomas Luxbacher, Fabien Serpaggi, Université de Versailles Saint-Quentin-en-Yvelines

B

Aniline Oligomers As a Model for Polyaniline: A Solid-State NMR Study. P. Michael Schmeida, Matthew Espe, University of Akron

A

Examples of Sodium and Gallium Chemical Shielding Anisotropy. Robert W. Schurko, Clare P. Grey, SUNY at Stony Brook; Roderick E. Wasylishen, Dalhousie University; Anthony Bielecki, Bruker Instruments, Inc.

B

Characterisation of Structure and Dynamics in Nanocrystalline Oxides by Solid State NMR. I.J.F. Poplett, M.E. Smith, University of Warwick; A.V. Chadwick and J.H. Strange, University of Kent

A

Multiple Quantum MAS NMR Experiments on I=5/2 Nuclei. M.E.Smith, R. Dupree and T. Mildner, University of Warwick; E.R.H. van Eck, University of Kent; S.C. Kohn, University of Bristol

B

Solid-State NMR Investigation of Leached Layers in Sodium-Aluminosilicate Glasses. Natia Tsomaia, James Hamilton, Karl T. Mueller, Penn State University

A

Comparative Study of Li-ion Mobility in Swollen Ionomers as Measured by 7Li MAS Lineshape, T1p, 7Li Diffusion, and Conductivity. A. J. Vega, E. F. McCord, M. Doyle and M. G. Roelofs, DuPont Central Research and Development

B

Dynamics of polarization transfer in high speed CPMAS experiments. Vladimir Ladizhansky and Shimon Vega, Weizmann Institute of Science

A

Residual Dipolar Couplings Between Quadrupolar Nuclei in Solid State MQMAS NMR Spectra. Sungsool Wi and Lucio Frydman, University of Illinois at Chicago

B

Measurements of Connectivities between PO4 Units in Zinc Phosphate Glasses. Jerzy W. Wiench, Marek Pruski, Brad Tischendorf, Joshua Otaigbe, Iowa State University

A

Deuterium Wide-line NMR Studies of Local Motion of Benzene Adsorbed on Ca-Montmorillonite. Jincheng Xiong, Union Carbide Corp.; Gary Maciel, Colorado State University

B

Probing Electronic and Protonation States In a Polymer: A 15N SSNMR Study of Polyaniline. Tanya Young, Matthew Espe,University of Akron; Dali Yang, Benjamin Mattes, Santa Fe Science and Technology

A

Investigation of Poly(lactide) Structure Using Solid-State NMR Spectroscopy, Mark T. Zell, Brian E. Padden, Amanda J. Paterick, Marc A. Hillmyer, Eric J. Munson, University of Minnesota; Khalid A.M. Thakur, Robert T. Kean, Cargill Incorporated

B

Solid-State27 A1 and 39Si NMR Investigations of Mg(II), Al(III) and Si(IV) Chemical Environments and Ordering in Various Montmorillonite Clay Minerals. John J. Fitzgerald, South Dakota State University; Don Eisenhour, American Colloid Company; Herman Lock, Gary E. Maciel, Colorado State University

A

Measurement of Diffusion Beyond NMR Imaging Spatial Resolution. Peter Trautner, Klaus Woelk and Joachim Bargon, University of Bonn

 

 

  

 
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